TA Instruments

AR1756-0011f

15/03/2013 15:12:01

Sample name	ASW Blank coupon#20 + DI + beads 50rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	11 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:12:01

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 50.00 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	50.00	181.12	10000	20.0	0.2153	1.004	59.04	62.50	0.9447	877.1	41.9763	0.2246	52.470	5247.0	3.411E-3	0.0	0.0
2.0200	50.00	34.634	10000	20.0	0.2183	2.020	11.29	62.50	0.1806	889.5	92.1582	0.2277	115.20	11520	3.411E-3	0.0	0.0
3.0240	50.00	34.968	10000	20.0	0.2167	3.024	11.40	62.50	0.1824	882.9	142.4250	0.2260	178.03	17803	3.411E-3	0.1	0.1
4.0280	50.00	34.877	10000	20.0	0.2143	4.028	11.37	62.50	0.1819	872.9	192.6740	0.2235	240.84	24084	3.411E-3	0.1	0.1
5.0200	50.00	34.799	10000	20.0	0.2165	5.020	11.34	62.50	0.1815	882.0	242.9610	0.2258	303.70	30370	3.411E-3	0.1	0.1
6.0080	50.00	34.513	10000	20.0	0.2209	6.008	11.25	62.50	0.1800	900.2	293.4570	0.2305	366.82	36682	3.411E-3	0.1	0.1
7.0040	50.00	34.996	10000	20.0	0.2173	7.004	11.41	62.50	0.1825	885.3	343.8860	0.2266	429.86	42986	3.411E-3	0.1	0.1
8.0040	50.00	35.228	10000	20.0	0.2191	8.004	11.48	62.50	0.1837	892.8	393.9690	0.2285	492.46	49246	3.411E-3	0.1	0.1
9.0040	50.00	34.878	10000	20.0	0.2171	9.004	11.37	62.50	0.1819	884.5	444.4780	0.2264	555.60	55560	3.411E-3	0.2	0.2
10.024	50.00	35.381	10000	20.0	0.2161	10.024	11.53	62.50	0.1845	880.4	494.7950	0.2254	618.49	61849	3.411E-3	0.2	0.2
11.024	50.00	35.395	10000	20.0	0.2193	11.024	11.54	62.50	0.1846	893.6	545.1210	0.2288	681.40	68140	3.411E-3	0.2	0.2
12.020	50.00	35.331	10000	20.0	0.2167	12.020	11.52	62.50	0.1843	882.9	594.9260	0.2260	743.66	74366	3.411E-3	0.2	0.2
13.020	50.00	35.971	10000	20.0	0.2155	13.020	11.72	62.50	0.1876	877.9	645.3700	0.2248	806.71	80671	3.411E-3	0.2	0.2
14.028	50.00	35.514	10000	20.0	0.2167	14.028	11.58	62.50	0.1852	882.9	695.6870	0.2260	869.61	86961	3.411E-3	0.2	0.2
15.024	50.00	35.432	10000	20.0	0.2169	15.024	11.55	62.50	0.1848	883.7	745.8090	0.2262	932.26	93226	3.411E-3	0.3	0.3
16.024	50.00	35.534	10000	20.0	0.2173	16.024	11.58	62.50	0.1853	885.3	796.4010	0.2266	995.50	99550	3.411E-3	0.3	0.3
17.020	50.00	35.600	10000	20.0	0.2151	17.020	11.60	62.50	0.1857	876.2	846.6310	0.2243	1058.3	1.0583E5	3.411E-3	0.3	0.3
18.024	50.00	35.525	10000	20.0	0.2151	18.024	11.58	62.50	0.1853	876.2	896.7980	0.2243	1121.0	1.1210E5	3.411E-3	0.3	0.3
19.028	50.00	35.647	10000	20.0	0.2165	19.028	11.62	62.50	0.1859	882.0	947.2140	0.2258	1184.0	1.1840E5	3.411E-3	0.3	0.3
20.028	50.00	35.669	10000	20.0	0.2147	20.028	11.63	62.50	0.1860	874.6	996.9220	0.2239	1246.2	1.2462E5	3.411E-3	0.3	0.3
21.024	50.00	35.989	10000	20.0	0.2169	21.024	11.73	62.50	0.1877	883.7	1047.4500	0.2262	1309.3	1.3093E5	3.411E-3	0.4	0.4
22.024	50.00	36.073	10000	20.0	0.2155	22.024	11.76	62.50	0.1881	877.9	1097.9399	0.2247	1372.4	1.3724E5	3.411E-3	0.4	0.4
23.020	50.00	35.846	10000	20.0	0.2143	23.020	11.68	62.50	0.1869	872.9	1147.7500	0.2235	1434.7	1.4347E5	3.411E-3	0.4	0.4
24.024	50.00	35.593	10000	20.0	0.2171	24.024	11.60	62.50	0.1856	884.5	1198.0200	0.2264	1497.5	1.4975E5	3.411E-3	0.4	0.4
25.024	50.00	35.761	10000	20.0	0.2183	25.024	11.66	62.50	0.1865	889.5	1248.2800	0.2277	1560.4	1.5604E5	3.411E-3	0.4	0.4
26.020	50.00	35.467	10000	20.0	0.2187	26.020	11.56	62.50	0.1850	891.1	1298.6500	0.2281	1623.3	1.6233E5	3.411E-3	0.4	0.4
27.020	50.00	35.652	10000	20.0	0.2161	27.020	11.62	62.50	0.1859	880.4	1348.8101	0.2254	1686.0	1.6860E5	3.411E-3	0.5	0.5
28.020	50.00	35.290	10000	20.0	0.2147	28.020	11.50	62.50	0.1840	874.6	1399.0800	0.2239	1748.9	1.7489E5	3.411E-3	0.5	0.5
29.028	50.00	35.938	10000	20.0	0.2191	29.028	11.71	62.50	0.1874	892.8	1449.5100	0.2286	1811.9	1.8119E5	3.411E-3	0.5	0.5
30.004	50.00	36.242	10000	20.0	0.2203	30.004	11.81	62.50	0.1890	897.7	1500.3101	0.2298	1875.4	1.8754E5	3.411E-3	0.5	0.5
31.024	50.00	36.141	10000	20.0	0.2193	31.024	11.78	62.50	0.1885	893.6	1549.9100	0.2288	1937.4	1.9374E5	3.411E-3	0.5	0.5
32.024	50.00	36.146	10000	20.0	0.2207	32.024	11.78	62.50	0.1885	899.4	1600.1300	0.2303	2000.2	2.0002E5	3.411E-3	0.5	0.5
33.024	50.00	36.055	10000	20.0	0.2159	33.024	11.75	62.50	0.1880	879.6	1650.6500	0.2252	2063.3	2.0633E5	3.411E-3	0.6	0.6
34.028	50.00	36.178	10000	20.0	0.2132	34.028	11.79	62.50	0.1887	868.8	1700.6600	0.2224	2125.8	2.1258E5	3.411E-3	0.6	0.6
35.024	50.00	35.902	10000	20.0	0.2132	35.024	11.70	62.50	0.1872	868.8	1750.9301	0.2224	2188.7	2.1887E5	3.411E-3	0.6	0.6
36.024	50.00	35.846	10000	20.0	0.2134	36.024	11.68	62.50	0.1869	869.6	1801.5800	0.2226	2252.0	2.2520E5	3.411E-3	0.6	0.6
37.024	50.00	35.932	10000	20.0	0.2149	37.024	11.71	62.50	0.1874	875.4	1851.4600	0.2241	2314.3	2.3143E5	3.411E-3	0.6	0.6
38.032	50.00	36.207	10000	20.0	0.2181	38.032	11.80	62.50	0.1888	888.7	1901.7200	0.2275	2377.2	2.3772E5	3.411E-3	0.6	0.6
39.032	50.00	36.236	10000	20.0	0.2181	39.032	11.81	62.50	0.1890	888.7	1952.2000	0.2275	2440.3	2.4403E5	3.411E-3	0.7	0.7
40.028	50.00	36.209	10000	20.0	0.2157	40.028	11.80	62.50	0.1888	878.7	2002.2900	0.2250	2502.9	2.5029E5	3.411E-3	0.7	0.7
41.020	50.00	35.663	10000	20.0	0.2134	41.020	11.62	62.50	0.1860	869.6	2052.5500	0.2226	2565.7	2.5657E5	3.411E-3	0.7	0.7
42.020	50.00	35.395	10000	20.0	0.2183	42.020	11.54	62.50	0.1846	889.5	2102.7800	0.2277	2628.5	2.6285E5	3.411E-3	0.7	0.7
43.028	50.00	35.828	10000	20.0	0.2183	43.028	11.68	62.50	0.1869	889.5	2153.6499	0.2277	2692.1	2.6921E5	3.411E-3	0.7	0.7
44.028	50.00	36.079	10000	20.0	0.2155	44.028	11.76	62.50	0.1882	877.9	2203.4399	0.2247	2754.3	2.7543E5	3.411E-3	0.7	0.7
45.004	50.00	36.242	10000	20.0	0.2193	45.004	11.81	62.50	0.1890	893.6	2253.8101	0.2288	2817.3	2.8173E5	3.411E-3	0.8	0.8
46.028	50.00	36.175	10000	20.0	0.2183	46.028	11.79	62.50	0.1887	889.5	2303.8999	0.2277	2879.9	2.8799E5	3.411E-3	0.8	0.8
47.024	50.00	36.054	10000	20.0	0.2195	47.024	11.75	62.50	0.1880	894.4	2354.7700	0.2290	2943.5	2.9435E5	3.411E-3	0.8	0.8
48.028	50.00	35.338	10000	20.0	0.2171	48.028	11.52	62.50	0.1843	884.5	2404.8701	0.2264	3006.1	3.0061E5	3.411E-3	0.8	0.8
49.032	50.00	35.212	10000	20.0	0.2181	49.032	11.48	62.50	0.1836	888.7	2455.3601	0.2275	3069.2	3.0692E5	3.411E-3	0.8	0.8
50.004	50.00	35.837	10000	20.0	0.2197	50.004	11.68	62.50	0.1869	895.3	2505.2000	0.2292	3131.5	3.1315E5	3.411E-3	0.8	0.8
51.020	50.00	36.261	10000	20.0	0.2199	51.020	11.82	62.50	0.1891	896.1	2555.4800	0.2294	3194.4	3.1944E5	3.411E-3	0.9	0.9
52.020	50.00	36.167	10000	20.0	0.2212	52.020	11.79	62.50	0.1886	901.1	2605.7100	0.2307	3257.1	3.2571E5	3.411E-3	0.9	0.9
53.020	50.00	35.837	10000	20.0	0.2179	53.020	11.68	62.50	0.1869	887.8	2630.5701	0.2273	3288.2	3.2882E5	3.411E-3	0.9	0.9
54.028	50.00	35.934	10000	20.0	0.2477	54.028	11.71	62.50	0.1874	1009	2706.4299	0.2584	3383.0	3.3830E5	3.411E-3	0.9	0.9
55.024	50.00	35.994	10000	20.0	0.2222	55.024	11.73	62.50	0.1877	905.2	2731.1001	0.2317	3413.9	3.4139E5	3.411E-3	0.9	0.9
56.016	50.00	36.105	10000	20.0	0.2185	56.016	11.77	62.50	0.1883	890.3	2781.3999	0.2279	3476.8	3.4768E5	3.411E-3	0.9	0.9
57.020	50.00	35.907	10000	20.0	0.2169	57.020	11.70	62.50	0.1873	883.7	2831.6399	0.2262	3539.6	3.5396E5	3.411E-3	1.0	1.0
58.024	50.00	35.507	10000	20.0	0.2145	58.024	11.57	62.50	0.1852	873.8	2907.5000	0.2237	3634.4	3.6344E5	3.411E-3	1.0	1.0
59.028	50.00	35.745	10000	20.0	0.2173	59.028	11.65	62.50	0.1864	885.3	2932.1799	0.2266	3665.2	3.6652E5	3.411E-3	1.0	1.0
60.020	50.00	35.451	10000	20.0	0.1370	60.020	11.56	62.50	0.1849	558.0	2982.4199	0.1428	3728.0	3.7280E5	3.411E-3	1.0	1.0

